Sunday, 12 November 2017

Clarification and Filtration Full Chapter PDF Free Download


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Filtration may be defined as the separation of solid from a fluid by means of a porous medium that retains the solid but allows the fluid to pass.

*The suspension of solid and liquid to be filtered is known as the slurry.
The porous medium used to retain the solids is described as the filter medium;
         The accumulation of solids on the filter is referred to as the filter cake,
         while the clear liquid passing through the filter is the filtrate.

Factors Affecting Filtration

         Filtration is affected by the characteristics of the slurry, including:
         1- The properties of the liquid , such as density, viscosity, and corrosiveness.
         2- The properties of the solid, for example, particle shape, particle size, particle size distribution, and the rigidity or compressibility of the solid.
         3- The proportion of solids in the slurry.
         4- Whether the objective is to collect the solid, the liquid ,or both.
         5- Whether the solids have to be washed free from the liquid or a solute.
         The surface upon which solids are deposited in a filter is called the Filter medium.

Filter Medium

         Properties of ideal filter medium: 
         1- It must be capable of delivering a clear filtrate at a suitable production rate.
         2- It must withstand the mechanical stresses without rupturing or being compressed.
         3- No chemical or physical interactions with the components of the filtrate should occur.
         4- It must retain the solids without plugging at the start of filtration.
         5-  Sterile filtration imposes a special requirement since the pore size must not exceed the dimension of bacteria or spores.


Types of Filter Medium

         1- Woven filters: these include  a- wire screening .         b- fabrics of cotton, wool, nylon.
            Wire screening e.g. stainless steel is durable, resistance to plugging and easily cleaned.
         Cotton is a common filter ,however, Nylon is superior for pharmaceutical use, since it is unaffected by mold, fungus or bacteria and has negligible absorption properties .
         2- Non- woven filters: Filter paper is a common filter medium since it offers controlled porosity, limited absorption characteristic, and low cost.
        3- Membrane filters: These are basic tools for micro-filtration, useful in the preparation of sterile solutions. These filters are made by casting of various esters of cellulose, or from nylon, Teflon, polyvinyl chloride. The filter is a thin membrane with millions of pores per square centimeter of filter surface.

        4-Porous plates:  These include perforated metal or rubber plates, natural porous materials such as stone, porcelain or ceramics, and sintered glass.

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